图2。(a)使用基于有机的(MEOH-DMSO)电解浴的循环伏安图在ITO底物上以10 mV.s-1的扫描速率记录。(b)选定的循环伏安法扫描后,Ni 3(HITP)2个沉积物的SEM图像。(C) The chronoamperograms (normalized current density) and the corresponding cumulative deposition charge density for potentiostatic anodic deposition methods by using the continuous (dark colored line) and square pulsed (light colored line) methods (with t on = 1 min, V on = 0.8 V; and t off = 1 min, V off = open circuit voltage).(d)Ni 3(HITP)2个沉积物的相应SEM图像通过电位连续(深色轮廓)和脉冲沉积(浅色轮廓)获得。
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